35 SEED TESTING INTERNATIONAL APRIL 2026 • RULES DEVELOPMENT markers tested in CT1. The markers were tested as three different marker systems/panels: one had four markers and the other two each had five markers. Each participant received ten tubes with subsamples and two tubes of pools of 40 crushed seeds per variety. Samples were provided in sealed tubes labelled with the name or code of the variety. Duplicates were provided to all participants as a backup. However, if any participating laboratory ran out of a sample, they were able to contact the CT leader to request more material. Equipment, Chemicals and Procedure Inclusion of DNA-based methods into the ISTA Rules is semi-performance-based. Laboratories were provided with guidelines for running the SSR prescribed, but the specific procedure was ultimately up to the participating laboratories. Evaluation and Reporting of Results Results were reported in an Excel spreadsheet indicating laboratory number, variety name, SSR name and allele sizes. Five of the six laboratories that participated in CT1 sent a data package. The data analysis from CT1 aimed to evaluate if the marker panel was reproducible among laboratories and thus suitable for being kept for CT2, and eventually for the ISTA Rules proposal. This evaluation was carried out by the crop leader and consisted of verifying if markers gave the same allele pattern across laboratories (even if different equipment and reagents were used). For CT2, the group leader compiled the results and prepared an Excel file with allele sizes and binary data. Binary data was sent to the Chair of the ISTA Statistics Committee for their analysis. All laboratories that participated in CT2 sent a data package. Statistical Analysis Overall percentage agreements (pα) and Cohen’s kappas have been computed for all the possible laboratory pairs, considering as units either the marker alleles or the varieties. The computations have been performed with the R irr package (Gamer et al., 2012), which includes functions for computing various coefficients of reliability of agreement. Within-laboratory agreement has been assessed through accordance as described in Langton et al. (2002). The average accordance across varieties is high in all the laboratories (above 95%) except in laboratory G (92.3%, when considering only individual seeds). Agreement of the marker results across laboratories has been assessed with Fleiss’ kappa κ on all the varieties except varieties 3 and 4. The agreement is perfect (κ=1) for all the varieties according to the Landis and Koch (1977) table for the interpretation of κ. The conclusion of the statistical analysis is that given these results, there is enough evidence for validating the method. Final Comments and Conclusions After running two CTs for barley varietal identification using a panel of 14 SSR markers and with the participation of ten laboratories from around the world, the statistical analysis done by the ISTA Statistics Committee concluded that there is enough evidence for validating the method for four SSR markers. Given the work carried out and the conclusion of the Statistics Committee, the ISTA Variety Committee presents this validation report for considering the inclusion of the barley SSR marker panel in the ISTA Rules, Chapter 8. References 1. Gamer, M., Lemon, J., Fellows, I. and Singh, P. (2012). Package ‘irr’: Various Coefficients of Interrater Reliability and Agreement. The Comprehensive R Archive Network, Vienna. 2. ISTA (2025). International Rules for Seed Testing. International Seed Testing Association, Wallisellen, Switzerland. 3. Langton, S.D., Chevennement, R., Nagelkerke, N. and Lombard, B. (2002). Analysing collaborative trials for qualitative microbiological methods: accordance and concordance. International Journal of Food Microbiology, 79, 175–181. 4. Landis, J.R. and Koch, G.G. (1977). The measurement of observer agreement for categorical data. Biometrics, 33, 159–174. 5. Perry, D.J., Fernando, U. and Lee, S.-J. (2013). Simple sequence repeat-based identification of Canadian malting barley varieties. Canadian Journal of Plant Science, 94, 485–496.
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