34 SEED TESTING INTERNATIONAL www.seedtest.org RULES DEVELOPMENT • Validation of a New Method for a ‘Microsatellite Marker Analysis for Barley Variety Verification’ Verena Peterseil1, Doris Kaiser1, Marie-Claude Gagnon2, Ana Laura Vicario3 and Sean Walkowiak4 1Austrian Agency for Health and Food Safety, Vienna, Austria 2Canadian Food Inspection Agency, Ottawa, Canada; ISTA Variety Committee Chair 3Instituto Nacional de Semillas INASE, Buenos Aires, Argentina; ISTA Variety Committee Vice-Chair 4Canadian Grain Commission, Winnipeg, Canada; ISTA Variety Committee Vice-Chair ISTA’S STANDARDISED PROCEDURES FOR THE DETERMINATION OF VARIETY VERIFICATION have traditionally been based on the examination of seeds, seedlings or plants in a laboratory, glasshouse, growth chamber or field plot, to assess morphology (grow-out tests), specific substances (biochemical methods) or protein characteristics (protein-based methods). DNA-based approaches are very useful tools for variety verification and for assessment of purity. In comparison to traditional variety verification methods, DNA-based techniques may reveal more polymorphism, thus allowing greater resolution among varieties. DNA- based techniques are also independent of environmental conditions or developmental stages. To initiate the process for the inclusion of a new DNA-based method for barley variety verification by means of microsatellite markers into the International Rules for Seed Testing (ISTA Rules), comparative test (CT) leader Verena Peterseil organised two CTs with the participation of laboratories from several countries around the world, over a period of three years. The objectives of the CTs carried out are summarised below: • The aim of CT1 was to compare results among participant laboratories and evaluate the possibility of obtaining the same simple sequence repeat (SSR) profiles and same allele sizes using different reagents, equipment and working protocols. Varieties and SSR markers were the same for all participant laboratories. The expected result of CT1 was to obtain comparable results among laboratories. • The aim of CT2 was also to compare results among participant laboratories and evaluate the possibility of obtaining the same SSR profile and same allele sizes when using different reagents, equipment and working protocols. Varieties and SSR markers were the same for all participant laboratories. • During CT2, the applicability of the method was evaluated by extending the range of varieties tested compared to CT1. In addition, reproducibility of the markers was tested through comparing the results of different laboratories with those of CT1. Repeatability was tested by using variety Semper which was also used in the first CT. Two out of a total of 12 laboratories participated in both CTs. Materials and Methods Samples For CT1, eight varieties (authorised in Austria) were analysed using ten SSR markers obtained from Perry et al. (2013) and four SSR markers developed by the Austrian Agency for Health and Food Safety (AGES; personal communication, Doris Kaiser and Verena Peterseil). Each participant received six individual crushed seeds per variety and two subsamples of a pool of 30–40 seeds. Samples were provided in sealed tubes labelled with the name or code of the variety. For CT2, nine varieties were analysed (four from Iran, two from Estonia, two from Lithuania and one from Austria) using the same 14 SSR
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